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Information card for entry 7037888
Preview
Coordinates | 7037888.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C12 H60 Fe2 N8 Na2 O88 Sb2 W20 |
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Calculated formula | C12 H20 Fe2 N8 Na2 O88 Sb2 W20 |
SMILES | [nH]1c[nH+]cc1.O=[W]123(O[W]456(O[W]789(O[W]%10%11(=O)(O4)O[W]4%12(=O)(O[W]%13%14%15(=[O][Fe]([O]=4)([O]=[W]4%16%17(O2)O[W]2%18%19(O[W]%20%21(O1)(O[W]1%22([O]%23%20[W]%20(=O)(O[W]%24%25%26(=O)=[O][Fe]([O]=%20)([OH2])([OH2])([OH2])[O]=[W]%20%27(O3)(O[W]3%28(O7)(O[W]7(O[W](=O)(O[W]%29%30(O[W]%31(O2)([O]%16%18[Sb]%23[O]%25%30[W](=O)(O%29)(O%31)(O1)O%24)(=O)O%17)(O%26)=O)(=O)(O%20)O4)([O]%13([Sb]([O]5%10%12)[O]9%273)[W](=O)(O7)(O%28)(O%11)O%14)(=O)O%15)=O)O8)(O%22)O%21)(=O)O%19)=O)=O)([OH2])([OH2])[OH2])=O)O6)=O)=O)=O.c1[nH]cc[nH+]1.O.O.[Na+].O.O.O.O.c1[nH]cc[nH+]1.O.[Na+].O.O.O.O.O.c1[nH]cc[nH+]1 |
Title of publication | Synthesis of [Sb2W20Fe(H2O)6O70](10-) with iron powder under mild conditions and its applications in both catalytic Fenton reaction and electrochemical sensing of ascorbic acid. |
Authors of publication | Sun, Minghui; Li, Fengyan; Yu, Longjiao; Wang, Ya; Xu, Lin |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 6 |
Pages of publication | 2417 - 2421 |
a | 13.017 ± 0.005 Å |
b | 13.539 ± 0.005 Å |
c | 17.702 ± 0.005 Å |
α | 68.517 ± 0.005° |
β | 79.923 ± 0.005° |
γ | 62.222 ± 0.005° |
Cell volume | 2568.4 ± 1.6 Å3 |
Cell temperature | 191 ± 2 K |
Ambient diffraction temperature | 191 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0794 |
Residual factor for significantly intense reflections | 0.0607 |
Weighted residual factors for significantly intense reflections | 0.1604 |
Weighted residual factors for all reflections included in the refinement | 0.1816 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7037888.html
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