Information card for entry 7037998

Structure parameters

• Formula: C55 H112 Ge9 K Si12
• Calculated formula: C55 H112 Ge9 K Si12
• Title of publication: {Ge9[Si(SiMe3)3]2}(2-): a starting point for mixed substituted metalloid germanium clusters.
• Authors of publication: Kysliak, O.; Schnepf, A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 6
• Pages of publication: 2404 - 2408
• a: 15.8387 ± 0.0009 Å
• b: 20.2949 ± 0.0013 Å
• c: 27.3283 ± 0.0016 Å
• α: 90°
• β: 91.293 ± 0.001°
• γ: 90°
• Cell volume: 8782.3 ± 0.9 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150.01 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.089
• Residual factor for significantly intense reflections: 0.062
• Weighted residual factors for significantly intense reflections: 0.1505
• Weighted residual factors for all reflections included in the refinement: 0.1638
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No