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Information card for entry 7038056
Preview
Coordinates | 7038056.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C70 H116 La2 N6 O6 Si4 |
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Calculated formula | C70 H116 La2 N6 O6 Si4 |
SMILES | C1(c2c(C)cc(cc2C)C)=[N]2CC(C)(C)C[N]3=C([O]4[La]567(N([Si](C)(C)C)[Si](C)(C)C)OC(c8c(cc(cc8C)C)C)=[N]6CC(C)(C)C[N]7=C([O]5[La]234(O1)N([Si](C)(C)C)[Si](C)(C)C)c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C.O1CCCC1.O1CCCC1 |
Title of publication | Synthesis and characterization of bridged bis(amidato) rare earth metal amides and their applications in C-N bond formation reactions. |
Authors of publication | Zhao, Bei; Xiao, Yang; Yuan, Dan; Lu, Chengrong; Yao, Yingming |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 9 |
Pages of publication | 3880 - 3887 |
a | 13.8887 ± 0.0003 Å |
b | 11.736 ± 0.0003 Å |
c | 24.6902 ± 0.0007 Å |
α | 90° |
β | 103.731 ± 0.003° |
γ | 90° |
Cell volume | 3909.43 ± 0.18 Å3 |
Cell temperature | 253 ± 2 K |
Ambient diffraction temperature | 253 ± 2 K |
Number of distinct elements | 6 |
Space group number | 13 |
Hermann-Mauguin space group symbol | P 1 2/c 1 |
Hall space group symbol | -P 2yc |
Residual factor for all reflections | 0.0542 |
Residual factor for significantly intense reflections | 0.0412 |
Weighted residual factors for significantly intense reflections | 0.1089 |
Weighted residual factors for all reflections included in the refinement | 0.1167 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.083 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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