Information card for entry 7038138

Structure parameters

• Formula: C33 H50 F6 N5 Ni Sb
• Calculated formula: C33 H50 F6 N5 Ni Sb
• Title of publication: Oxidatively-induced aromatic cyanation mediated by Ni(iii).
• Authors of publication: Zhou, Wen; Rath, Nigam P.; Mirica, Liviu M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 21
• Pages of publication: 8693 - 8695
• a: 26.184 ± 0.003 Å
• b: 15.0342 ± 0.0015 Å
• c: 20.694 ± 0.002 Å
• α: 90°
• β: 115.048 ± 0.011°
• γ: 90°
• Cell volume: 7380.2 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1584
• Residual factor for significantly intense reflections: 0.1056
• Weighted residual factors for significantly intense reflections: 0.2435
• Weighted residual factors for all reflections included in the refinement: 0.2688
• Goodness-of-fit parameter for all reflections included in the refinement: 1.375
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No