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Information card for entry 7038142
Preview
Coordinates | 7038142.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Binolphosphine |
---|---|
Formula | C36 H55 N4 O P Si3 Zr |
Calculated formula | C36 H55 N4 O P Si3 Zr |
SMILES | [Zr]123([P]c4c(c5c(OC)ccc6c5cccc6)c5c(cc4)cccc5)[N](CCN3[Si](C)(C)C)(CCN1[Si](C)(C)C)CCN2[Si](C)(C)C |
Title of publication | Zirconium-catalyzed intermolecular hydrophosphination using a chiral, air-stable primary phosphine. |
Authors of publication | Bange, Christine A.; Ghebreab, Michael B.; Ficks, Arne; Mucha, Neil T.; Higham, Lee; Waterman, Rory |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 5 |
Pages of publication | 1863 - 1867 |
a | 10.843 ± 0.002 Å |
b | 12.324 ± 0.002 Å |
c | 18.699 ± 0.003 Å |
α | 77.714 ± 0.002° |
β | 81.478 ± 0.002° |
γ | 71.588 ± 0.002° |
Cell volume | 2307.7 ± 0.7 Å3 |
Cell temperature | 128 ± 2 K |
Ambient diffraction temperature | 128 ± 2 K |
Number of distinct elements | 7 |
Space group number | 1 |
Hermann-Mauguin space group symbol | P 1 |
Hall space group symbol | P 1 |
Residual factor for all reflections | 0.0606 |
Residual factor for significantly intense reflections | 0.0485 |
Weighted residual factors for significantly intense reflections | 0.1255 |
Weighted residual factors for all reflections included in the refinement | 0.1327 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
Diffraction radiation wavelength | 0.71073 Å |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7038142.html
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