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Information card for entry 7038345
Preview
Coordinates | 7038345.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C48.5 H64.5 B2 F2 Fe N6 O10 P2 S2 |
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Calculated formula | C42.5 H50.5 B2 F2 Fe N6 O10 P2 S2 |
Title of publication | Clathrochelates meet phosphorus. New thio- and phosphorylation reactions of an iron(ii) dichloroclathrochelate precursor and preparation of its first phosphorus(iii)-containing macrobicyclic derivative. |
Authors of publication | Artyushin, Oleg I.; Matveeva, Ekaterina V.; Vologzhanina, Anna V.; Voloshin, Yan Z. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 12 |
Pages of publication | 5328 - 5333 |
a | 38.5967 ± 0.0016 Å |
b | 38.5967 ± 0.0016 Å |
c | 23.9936 ± 0.0015 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 30955 ± 3 Å3 |
Cell temperature | 120 K |
Ambient diffraction temperature | 120 K |
Number of distinct elements | 9 |
Space group number | 148 |
Hermann-Mauguin space group symbol | R -3 |
Hall space group symbol | -R 3 |
Residual factor for all reflections | 0.0714 |
Residual factor for significantly intense reflections | 0.0635 |
Weighted residual factors for significantly intense reflections | 0.1746 |
Weighted residual factors for all reflections included in the refinement | 0.182 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.098 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7038345.html
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