Information card for entry 7038474

Structure parameters

• Formula: C43.5 H40 B Cl3 F4 N O3 P3 W
• Calculated formula: C42 H37 B F4 N O3 P3 W
• Title of publication: Insight into the stereoelectronic parameters of N-triphos ligands via coordination to tungsten(0).
• Authors of publication: Phanopoulos, Andreas; White, Andrew J. P.; Long, Nicholas J.; Miller, Philip W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 13
• Pages of publication: 5536 - 5548
• a: 18.1122 ± 0.0004 Å
• b: 35.0113 ± 0.0008 Å
• c: 13.3447 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8462.3 ± 0.3 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 9
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0961
• Residual factor for significantly intense reflections: 0.0761
• Weighted residual factors for significantly intense reflections: 0.1602
• Weighted residual factors for all reflections included in the refinement: 0.1669
• Goodness-of-fit parameter for all reflections included in the refinement: 1.139
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No