Information card for entry 7038489

Structure parameters

• Formula: C36 H61 Bi2 Cl3 N3 Si3
• Calculated formula: C36 H61 Bi2 Cl3 N3 Si3
• Title of publication: Synthesis of mono-, di-, and triaminobismuthanes and observation of C-C coupling of aromatic systems with bismuth(iii) chloride.
• Authors of publication: Hering-Junghans, Christian; Schulz, Axel; Thomas, Max; Villinger, Alexander
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6053 - 6059
• a: 41.0217 ± 0.0014 Å
• b: 9.1798 ± 0.0003 Å
• c: 24.3117 ± 0.0009 Å
• α: 90°
• β: 90.767 ± 0.003°
• γ: 90°
• Cell volume: 9154.3 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0716
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0587
• Weighted residual factors for all reflections included in the refinement: 0.0673
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No