Information card for entry 7038498

Structure parameters

• Formula: C21 H38 Bi Cl2 N Si
• Calculated formula: C21 H38 Bi Cl2 N Si
• Title of publication: Synthesis of mono-, di-, and triaminobismuthanes and observation of C-C coupling of aromatic systems with bismuth(iii) chloride.
• Authors of publication: Hering-Junghans, Christian; Schulz, Axel; Thomas, Max; Villinger, Alexander
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6053 - 6059
• a: 25.691 ± 0.0007 Å
• b: 20.0014 ± 0.0005 Å
• c: 29.9643 ± 0.0008 Å
• α: 90°
• β: 90.167 ± 0.002°
• γ: 90°
• Cell volume: 15397.3 ± 0.7 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1585
• Residual factor for significantly intense reflections: 0.0591
• Weighted residual factors for significantly intense reflections: 0.0952
• Weighted residual factors for all reflections included in the refinement: 0.1231
• Goodness-of-fit parameter for all reflections included in the refinement: 0.96
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No