Information card for entry 7038550

Structure parameters

• Formula: C56 H62 B2 F24 N P2 Rh
• Calculated formula: C56 H62 B2 F24 N P2 Rh
• Title of publication: Variable coordination modes and catalytic dehydrogenation of B-phenyl amine-boranes.
• Authors of publication: Kumar, Amit; Priest, Isobel K.; Hooper, Thomas N.; Weller, Andrew S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6183 - 6195
• a: 25.1599 ± 0.0002 Å
• b: 18.7874 ± 0.0001 Å
• c: 26.2494 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12407.8 ± 0.15 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.1141
• Weighted residual factors for all reflections included in the refinement: 0.1216
• Goodness-of-fit parameter for all reflections included in the refinement: 0.787
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No