Information card for entry 7038627

Structure parameters

• Formula: C49 H64 Ag2 Cl2 F12 P2 Sb2
• Calculated formula: C49 H64 Ag2 Cl2 F12 P2 Sb2
• Title of publication: Multinuclear silver(i) XPhos complexes with cyclooctatetraene: photochemical C-C bond cleavage of acetonitrile and cyanide bridged Ag cluster formation.
• Authors of publication: Grirrane, A.; Álvarez, E; Albero, J.; García, H; Corma, A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 13
• Pages of publication: 5444 - 5450
• a: 21.7571 ± 0.0019 Å
• b: 10.1105 ± 0.0009 Å
• c: 26.215 ± 0.002 Å
• α: 90°
• β: 100.802 ± 0.002°
• γ: 90°
• Cell volume: 5664.5 ± 0.8 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0346
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.0777
• Weighted residual factors for all reflections included in the refinement: 0.0784
• Goodness-of-fit parameter for all reflections included in the refinement: 1.147
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No