Information card for entry 7038705

Structure parameters

• Common name: 2-Gd
• Chemical name: [(C5Me4H)2(THF)Gd]2(μ-η2:η2-N2)
• Formula: C58 H84 Gd2 N2 O2
• Calculated formula: C58 H82 Gd2 N2 O2
• Title of publication: Raman spectroscopy of the N-N bond in rare earth dinitrogen complexes.
• Authors of publication: Fieser, Megan E.; Woen, David H.; Corbey, Jordan F.; Mueller, Thomas J.; Ziller, Joseph W.; Evans, William J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 37
• Pages of publication: 14634 - 14644
• a: 15.2453 ± 0.0007 Å
• b: 13.9938 ± 0.0006 Å
• c: 25.6281 ± 0.0011 Å
• α: 90°
• β: 104.773 ± 0.0004°
• γ: 90°
• Cell volume: 5286.7 ± 0.4 ų
• Cell temperature: 88 ± 2 K
• Ambient diffraction temperature: 88 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0229
• Residual factor for significantly intense reflections: 0.019
• Weighted residual factors for significantly intense reflections: 0.0425
• Weighted residual factors for all reflections included in the refinement: 0.0449
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No