Information card for entry 7038825

Structure parameters

• Formula: C34 H41 B N2 Ni O4
• Calculated formula: C34 H41 B N2 Ni O4
• Title of publication: Direct C-C coupling of two Ni-salphen complexes to yield dinickel-disalphen complexes with symmetric and non-symmetric substitution-patterns.
• Authors of publication: Bugenhagen, B. E. C.; Prosenc, M. H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 17
• Pages of publication: 7460 - 7468
• a: 14.4687 ± 0.0001 Å
• b: 24.9127 ± 0.0002 Å
• c: 17.5423 ± 0.0002 Å
• α: 90°
• β: 92.753 ± 0.001°
• γ: 90°
• Cell volume: 6315.9 ± 0.1 ų
• Cell temperature: 100.1 ± 1 K
• Ambient diffraction temperature: 100.1 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.062
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.0883
• Weighted residual factors for all reflections included in the refinement: 0.1025
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No