Information card for entry 7038828

Structure parameters

• Common name: tBu-Ni-tBu-Ni-Bip
• Chemical name: tBu-Ni-tBu-Ni-Bip
• Formula: C64 H58 N6 Ni2 O4
• Calculated formula: C64 H58 N6 Ni2 O4
• Title of publication: Direct C-C coupling of two Ni-salphen complexes to yield dinickel-disalphen complexes with symmetric and non-symmetric substitution-patterns.
• Authors of publication: Bugenhagen, B. E. C.; Prosenc, M. H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 17
• Pages of publication: 7460 - 7468
• a: 16.4203 ± 0.0002 Å
• b: 8.0156 ± 0.0001 Å
• c: 20.0126 ± 0.0003 Å
• α: 90°
• β: 100.66°
• γ: 90°
• Cell volume: 2588.57 ± 0.06 ų
• Cell temperature: 100.15 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0682
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.0968
• Weighted residual factors for all reflections included in the refinement: 0.1092
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No