Information card for entry 7038956

Structure parameters

• Formula: C24 H64 Fe2 N2 P8
• Calculated formula: C24 H64 Fe2 N2 P8
• Title of publication: Teaching old compounds new tricks: efficient N2 fixation by simple Fe(N2)(diphosphine)2 complexes.
• Authors of publication: Doyle, Laurence R.; Hill, Peter J.; Wildgoose, Gregory G.; Ashley, Andrew E.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 18
• Pages of publication: 7550 - 7554
• a: 9.345 ± 0.0004 Å
• b: 9.6733 ± 0.0003 Å
• c: 23.4652 ± 0.001 Å
• α: 90.674 ± 0.003°
• β: 90.671 ± 0.004°
• γ: 115.639 ± 0.003°
• Cell volume: 1911.86 ± 0.14 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0556
• Residual factor for significantly intense reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.09
• Weighted residual factors for all reflections included in the refinement: 0.0984
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No