Information card for entry 7038979

Structure parameters

• Formula: C95 H123 Ge2 O2
• Calculated formula: C95 H123 Ge2 O2
• Title of publication: Addition of alkynes to digermynes: experimental insight into the reaction pathway.
• Authors of publication: Tashkandi, Nada Y.; Pavelka, Laura C.; Caputo, Christine A.; Boyle, Paul D.; Power, Philip P.; Baines, Kim M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 17
• Pages of publication: 7226 - 7230
• a: 12.871 ± 0.007 Å
• b: 16.645 ± 0.01 Å
• c: 23.354 ± 0.013 Å
• α: 71.593 ± 0.014°
• β: 87.449 ± 0.007°
• γ: 67.404 ± 0.008°
• Cell volume: 4366 ± 4 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0915
• Residual factor for significantly intense reflections: 0.0532
• Weighted residual factors for significantly intense reflections: 0.1288
• Weighted residual factors for all reflections included in the refinement: 0.1487
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No