Information card for entry 7038986

Structure parameters

• Chemical name: Ni(dmpbz)2(BF4)2
• Formula: C20 H32 B2 F8 Ni P4
• Calculated formula: C20 H32 B2 F8 Ni P4
• Title of publication: Solvent influence on the thermodynamics for hydride transfer from bis(diphosphine) complexes of nickel.
• Authors of publication: Connelly Robinson, Samantha J.; Zall, Christopher M.; Miller, Deanna L.; Linehan, John C.; Appel, Aaron M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 24
• Pages of publication: 10017 - 10023
• a: 16.0457 ± 0.0014 Å
• b: 9.2602 ± 0.0008 Å
• c: 17.5605 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2609.3 ± 0.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.1166
• Residual factor for significantly intense reflections: 0.0548
• Weighted residual factors for significantly intense reflections: 0.1244
• Weighted residual factors for all reflections included in the refinement: 0.1561
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No