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Information card for entry 7039020
Preview
Coordinates | 7039020.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C54 H75 Cl2 Ge P Sn |
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Calculated formula | C54 H75 Cl2 Ge P Sn |
SMILES | [Sn]1([Ge](Cl)[P](c2c1cccc2)(C1CCCCC1)C1CCCCC1)(Cl)c1c(cccc1c1c(C(C)C)cc(C(C)C)cc1C(C)C)c1c(cc(C(C)C)cc1C(C)C)C(C)C |
Title of publication | Reaction of stannylene phosphorus Lewis pairs with dichlorides of germanium, tin and lead - the formation of base stabilized stannyl stannylenes/germylenes and redox reaction with PbCl2. |
Authors of publication | Krebs, K. M.; Maudrich, J.-J.; Wesemann, L. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 19 |
Pages of publication | 8081 - 8088 |
a | 16.0516 ± 0.0004 Å |
b | 24.7557 ± 0.0006 Å |
c | 25.955 ± 0.0007 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 10313.7 ± 0.5 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0496 |
Residual factor for significantly intense reflections | 0.0308 |
Weighted residual factors for significantly intense reflections | 0.0606 |
Weighted residual factors for all reflections included in the refinement | 0.0663 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7039020.html
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