Information card for entry 7039022

Structure parameters

• Formula: C68 H80 Cl2 Ge P Sn
• Calculated formula: C68 H80 Cl2 Ge P Sn
• Title of publication: Reaction of stannylene phosphorus Lewis pairs with dichlorides of germanium, tin and lead - the formation of base stabilized stannyl stannylenes/germylenes and redox reaction with PbCl2.
• Authors of publication: Krebs, K. M.; Maudrich, J.-J.; Wesemann, L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 19
• Pages of publication: 8081 - 8088
• a: 29.0011 ± 0.0011 Å
• b: 19.7482 ± 0.0007 Å
• c: 10.5468 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6040.4 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0304
• Residual factor for significantly intense reflections: 0.0276
• Weighted residual factors for significantly intense reflections: 0.0623
• Weighted residual factors for all reflections included in the refinement: 0.0633
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No