Information card for entry 7039024

Structure parameters

• Formula: C60 H75 Cl2 P Sn
• Calculated formula: C60 H75 Cl2 P Sn
• SMILES: [Sn](Cl)(Cl)(c1c(cccc1c1c(cc(C(C)C)cc1C(C)C)C(C)C)c1c(cc(cc1C(C)C)C(C)C)C(C)C)c1c(P(c2ccccc2)c2ccccc2)cccc1.C=CCCCC
• Title of publication: Reaction of stannylene phosphorus Lewis pairs with dichlorides of germanium, tin and lead - the formation of base stabilized stannyl stannylenes/germylenes and redox reaction with PbCl2.
• Authors of publication: Krebs, K. M.; Maudrich, J.-J.; Wesemann, L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 19
• Pages of publication: 8081 - 8088
• a: 14.7617 ± 0.0003 Å
• b: 24.9093 ± 0.0005 Å
• c: 29.069 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10688.8 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.052
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.0782
• Weighted residual factors for all reflections included in the refinement: 0.0858
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No