Information card for entry 7039175

Structure parameters

• Formula: C23 H46 O7 W
• Calculated formula: C22.988 H45.976 O7 W
• Title of publication: Synthesis and evaluation of κ(2)-β-diketonate and β-ketoesterate tungsten(vi) oxo-alkoxide complexes as precursors for chemical vapor deposition of WOx thin films.
• Authors of publication: Bonsu, Richard O.; Bock, Duane C.; Kim, Hankook; Korotkov, Roman Y.; Abboud, Khalil A.; Anderson, Timothy J.; McElwee-White, Lisa
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 27
• Pages of publication: 10897 - 10908
• a: 9.7653 ± 0.0005 Å
• b: 17.3223 ± 0.0009 Å
• c: 17.2212 ± 0.0009 Å
• α: 90°
• β: 101.504 ± 0.001°
• γ: 90°
• Cell volume: 2854.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0447
• Residual factor for significantly intense reflections: 0.025
• Weighted residual factors for significantly intense reflections: 0.0498
• Weighted residual factors for all reflections included in the refinement: 0.0547
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No