Information card for entry 7039306

Structure parameters

• Formula: C30 H60 Ag2 B2 F8 P4
• Calculated formula: C30 H60 Ag2 B2 F8 P4
• Title of publication: Selective formation of silver(i) bis-phospholane macrocycles and further evidence that gold(i) is smaller than silver(i).
• Authors of publication: Streitberger, Markus; Schmied, Andy; Hoy, Reinhard; Hey-Hawkins, Evamarie
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 29
• Pages of publication: 11644 - 11649
• a: 9.017 ± 0.005 Å
• b: 17.562 ± 0.005 Å
• c: 12.399 ± 0.005 Å
• α: 90 ± 0.005°
• β: 97.526 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 1946.5 ± 1.4 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0358
• Residual factor for significantly intense reflections: 0.0282
• Weighted residual factors for significantly intense reflections: 0.0609
• Weighted residual factors for all reflections included in the refinement: 0.064
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No