Information card for entry 7039348

Structure parameters

• Formula: C18 H18 F6 N5 O Pd Sb
• Calculated formula: C18 H18 F6 N5 O Pd Sb
• Title of publication: Divergent reactivity of platinum(ii) and palladium(ii) methylperoxo complexes and the formation of an unusual hemi-aminal complex.
• Authors of publication: Petersen, Allan R.; White, Andrew J. P.; Britovsek, George J. P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 37
• Pages of publication: 14520 - 14523
• a: 12.8162 ± 0.0003 Å
• b: 8.13176 ± 0.00016 Å
• c: 20.6429 ± 0.0005 Å
• α: 90°
• β: 100.132 ± 0.002°
• γ: 90°
• Cell volume: 2117.82 ± 0.08 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0436
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0642
• Weighted residual factors for all reflections included in the refinement: 0.0693
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No