Information card for entry 7039404

Structure parameters

• Formula: C35.5 H55.5 Fe N2 P
• Calculated formula: C35.5 H55.5 Fe N2 P
• Title of publication: Low coordinate iron derivatives stabilized by a β-diketiminate mimic. Synthesis and coordination chemistry of enamidophosphinimine scaffolds to generate diiron dinitrogen complexes.
• Authors of publication: Hein, Nicholas M.; Suzuki, Tatsuya; Ogawa, Takahiko; Fryzuk, Michael D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 37
• Pages of publication: 14697 - 14708
• a: 26.34 ± 0.003 Å
• b: 11.8226 ± 0.0016 Å
• c: 24.864 ± 0.003 Å
• α: 90°
• β: 106.786 ± 0.003°
• γ: 90°
• Cell volume: 7412.9 ± 1.6 ų
• Cell temperature: 90 K
• Ambient diffraction temperature: 90.15 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1488
• Residual factor for significantly intense reflections: 0.1319
• Weighted residual factors for significantly intense reflections: 0.3467
• Weighted residual factors for all reflections included in the refinement: 0.3535
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No