Crystallography Open Database

Information card for entry 7039448

Preview

Coordinates	7039448.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H54 N6 P3 Sb
Calculated formula	C30 H54 N6 P3 Sb
Title of publication	Paddlewheel 1,2,4-diazaphospholide distibines with the shortest antimony-antimony single bonds.
Authors of publication	Zhao, Minggang; Wang, Lixia; Zhang, Xiang; Zheng, Wenjun
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	26
Pages of publication	10505 - 10509
a	10.0959 ± 0.0005 Å
b	11.0582 ± 0.0004 Å
c	17.7867 ± 0.0006 Å
α	81.355 ± 0.003°
β	76.325 ± 0.003°
γ	79.091 ± 0.004°
Cell volume	1882.96 ± 0.14 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0544
Residual factor for significantly intense reflections	0.0395
Weighted residual factors for significantly intense reflections	0.0712
Weighted residual factors for all reflections included in the refinement	0.0782
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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