Information card for entry 7039452

Structure parameters

• Formula: C63 H96 N8 P4 Sb2
• Calculated formula: C63 H96 N8 P4 Sb2
• Title of publication: Paddlewheel 1,2,4-diazaphospholide distibines with the shortest antimony-antimony single bonds.
• Authors of publication: Zhao, Minggang; Wang, Lixia; Zhang, Xiang; Zheng, Wenjun
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 26
• Pages of publication: 10505 - 10509
• a: 10.913 ± 0.0003 Å
• b: 11.8061 ± 0.0003 Å
• c: 16.0228 ± 0.0004 Å
• α: 102.33 ± 0.002°
• β: 106.292 ± 0.002°
• γ: 104.337 ± 0.002°
• Cell volume: 1828.71 ± 0.09 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.1216
• Weighted residual factors for all reflections included in the refinement: 0.1307
• Goodness-of-fit parameter for all reflections included in the refinement: 1.097
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No