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Information card for entry 7039472
Preview
Coordinates | 7039472.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H20 Co N6 |
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Calculated formula | C24 H20 Co N6 |
SMILES | c12cccc[n]1[Co]1([n]3c(C=NN1c1ccccc1)cccc3)N(c1ccccc1)N=C2 |
Title of publication | Coordination reactions of 2-pyridinecarboxaldehyde-phenylhydrazonatolithium with selected transition metal (Zn, Sn, Fe, Co, Ni and Zr) chlorides and its coupling reaction with dichloromethane. |
Authors of publication | Duan, Xin-E; Tong, Hong-Bo; Wei, Xue-Hong; Shi, He-Ping; Bai, Sheng-Di; Bai, Tao; Zhang, Jing; Zhang, Yong-Bin; Liu, Dian-Sheng |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 27 |
Pages of publication | 11061 - 11070 |
a | 17.9 ± 0.004 Å |
b | 9.54 ± 0.0019 Å |
c | 12.45 ± 0.003 Å |
α | 90° |
β | 100.9 ± 0.03° |
γ | 90° |
Cell volume | 2087.7 ± 0.8 Å3 |
Cell temperature | 238 ± 2 K |
Ambient diffraction temperature | 238 ± 2 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0723 |
Residual factor for significantly intense reflections | 0.0511 |
Weighted residual factors for significantly intense reflections | 0.1257 |
Weighted residual factors for all reflections included in the refinement | 0.1417 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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