Information card for entry 7039696

Structure parameters

• Chemical name: (NHSi)Fe(N{SiMe3}2)2
• Formula: C83 H152 Fe2 N8 Si10
• Calculated formula: C83 H152 Fe2 N8 Si10
• Title of publication: A three-coordinate iron-silylene complex stabilized by ligand-ligand dispersion forces.
• Authors of publication: Hänninen, Mikko M; Pal, Kuntal; Day, Benjamin M.; Pugh, Thomas; Layfield, Richard A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 28
• Pages of publication: 11301 - 11305
• a: 11.3552 ± 0.0004 Å
• b: 12.5187 ± 0.0004 Å
• c: 18.5545 ± 0.0006 Å
• α: 78.705 ± 0.003°
• β: 89.821 ± 0.003°
• γ: 75.266 ± 0.003°
• Cell volume: 2498.4 ± 0.15 ų
• Cell temperature: 150.01 ± 0.13 K
• Ambient diffraction temperature: 150.01 ± 0.13 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0624
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.0958
• Weighted residual factors for all reflections included in the refinement: 0.1057
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No