Information card for entry 7040048

Structure parameters

• Common name: 4-OTf
• Chemical name: [{(AuLF)2(μ-OH)}2](OTf)2
• Formula: C74 H48 Au4 F18 O8 P4 S2
• Calculated formula: C74 H48 Au4 F18 O8 P4 S2
• Title of publication: The effect of counteranions on the molecular structures of phosphanegold(i) cluster cations formed by polyoxometalate (POM)-mediated clusterization.
• Authors of publication: Nagashima, Eri; Yoshida, Takuya; Matsunaga, Satoshi; Nomiya, Kenji
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 34
• Pages of publication: 13565 - 13575
• a: 15.9305 ± 0.0003 Å
• b: 15.9305 ± 0.0003 Å
• c: 17.083 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4335.3 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for all reflections: 0.0647
• Residual factor for significantly intense reflections: 0.0522
• Weighted residual factors for significantly intense reflections: 0.1505
• Weighted residual factors for all reflections included in the refinement: 0.1586
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No