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Information card for entry 7040109
Preview
Coordinates | 7040109.cif |
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Original paper (by DOI) | HTML |
Formula | C51 H29 B F24 Fe N3 Pd0.5 |
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Calculated formula | C51 H29 B F25.438 Fe N3 Pd0.5 |
Title of publication | Novel pyrazolylphosphite- and pyrazolylphosphinite-ruthenium(ii) complexes as catalysts for hydrogenation of acetophenone. |
Authors of publication | Amenuvor, Gershon; Obuah, Collins; Nordlander, Ebbe; Darkwa, James |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 34 |
Pages of publication | 13514 - 13524 |
a | 13.353 ± 0.0011 Å |
b | 13.7363 ± 0.0012 Å |
c | 14.4942 ± 0.0012 Å |
α | 86.401 ± 0.004° |
β | 83.876 ± 0.005° |
γ | 70.096 ± 0.004° |
Cell volume | 2484.5 ± 0.4 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 99.99 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0633 |
Residual factor for significantly intense reflections | 0.0556 |
Weighted residual factors for significantly intense reflections | 0.162 |
Weighted residual factors for all reflections included in the refinement | 0.1688 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.112 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7040109.html
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