Information card for entry 7040239

Structure parameters

• Formula: C56 H46 Cl2 Ge2 N4 O P2 Pd2 S4
• Calculated formula: C53.48 H43.93 Cl2 Ge2.013 N3.82 O P2 Pd2.013 S4
• Title of publication: Group 10-group 14 metal complexes [E-TM](IV): the role of the group 14 site as an L, X and Z-type ligand.
• Authors of publication: Wächtler, Erik; Gericke, Robert; Brendler, Erica; Gerke, Birgit; Langer, Thorsten; Pöttgen, Rainer; Zhechkov, Lyuben; Heine, Thomas; Wagler, Jörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 36
• Pages of publication: 14252 - 14264
• a: 9.5367 ± 0.0002 Å
• b: 22.055 ± 0.0004 Å
• c: 26.8568 ± 0.0006 Å
• α: 90°
• β: 96.955 ± 0.002°
• γ: 90°
• Cell volume: 5607.3 ± 0.2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0542
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0857
• Weighted residual factors for all reflections included in the refinement: 0.0916
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No