Information card for entry 7040259

Structure parameters

• Formula: C138 H131 Ag3 B3 N36
• Calculated formula: C138 H131 Ag3 B3 N36
• Title of publication: Ruthenium(ii) complexes of hemilabile pincer ligands: synthesis and catalysing the transfer hydrogenation of ketones.
• Authors of publication: Nair, Ashwin G.; McBurney, Roy T.; Walker, D. Barney; Page, Michael J.; Gatus, Mark R. D.; Bhadbhade, Mohan; Messerle, Barbara A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 36
• Pages of publication: 14335 - 14342
• a: 14.4586 ± 0.0006 Å
• b: 19.1802 ± 0.0007 Å
• c: 24.5632 ± 0.001 Å
• α: 99.448 ± 0.002°
• β: 99.315 ± 0.002°
• γ: 106.299 ± 0.002°
• Cell volume: 6291.9 ± 0.4 ų
• Cell temperature: 149.99 K
• Ambient diffraction temperature: 149.99 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0916
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.0963
• Weighted residual factors for all reflections included in the refinement: 0.1165
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No