Information card for entry 7040665

Structure parameters

• Formula: C136 H130 Cl30 I9 N15 O33 Pd3
• Calculated formula: C134 H128 Cl24 I9 N12 O24 Pd3
• Title of publication: Recyclable scavengers for photo-cyclopropanation via an in situ crystallization process.
• Authors of publication: Lee, Haeri; Choi, Eunkyung; Noh, Tae Hwan; Jung, Ok-Sang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 46
• Pages of publication: 18476 - 18483
• a: 14.029 ± 0.003 Å
• b: 41.786 ± 0.008 Å
• c: 37.004 ± 0.006 Å
• α: 90°
• β: 94.315 ± 0.009°
• γ: 90°
• Cell volume: 21631 ± 7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.3026
• Residual factor for significantly intense reflections: 0.1314
• Weighted residual factors for significantly intense reflections: 0.3742
• Weighted residual factors for all reflections included in the refinement: 0.4415
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No