Crystallography Open Database

Information card for entry 7040679

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Coordinates	7040679.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H44 B F24 N P2
Calculated formula	C65 H44 B F24 N P2
Title of publication	Donor-substituted phosphanes - surprisingly weak Lewis donors for phosphenium cation stabilisation.
Authors of publication	Clark, Ewan R.; Borys, Andryj M.; Pearce, Kyle
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	41
Pages of publication	16125 - 16129
a	13.06366 ± 0.00017 Å
b	13.20669 ± 0.00016 Å
c	19.4224 ± 0.0002 Å
α	103.87 ± 0.0011°
β	107.304 ± 0.0011°
γ	91.5968 ± 0.001°
Cell volume	3088.12 ± 0.07 Å³
Cell temperature	150 ± 1 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0781
Residual factor for significantly intense reflections	0.0691
Weighted residual factors for significantly intense reflections	0.1847
Weighted residual factors for all reflections included in the refinement	0.193
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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