Information card for entry 7041062

Structure parameters

• Formula: C34 H45 Li O3 Si
• Calculated formula: C34 H45 Li O3 Si
• Title of publication: Synthesis and study of an unprecedented 1-hydro-1-lithio-1-silafluorene anion.
• Authors of publication: Tian, Dawei; Li, Xiaofei; Liu, YuanYuan; Cao, Yue; Li, Tianhao; Hu, Hongfan; Cui, Chunming
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 46
• Pages of publication: 18447 - 18449
• a: 8.991 ± 0.004 Å
• b: 16.122 ± 0.007 Å
• c: 22.047 ± 0.01 Å
• α: 90°
• β: 91.154 ± 0.007°
• γ: 90°
• Cell volume: 3195 ± 2 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1173
• Residual factor for significantly intense reflections: 0.0994
• Weighted residual factors for significantly intense reflections: 0.2372
• Weighted residual factors for all reflections included in the refinement: 0.25
• Goodness-of-fit parameter for all reflections included in the refinement: 1.148
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No