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Information card for entry 7041380
Preview
Coordinates | 7041380.cif |
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Original paper (by DOI) | HTML |
Formula | C17 H15 Cl F6 N7 Ni P |
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Calculated formula | C17 H15 Cl F6 N7 Ni P |
Title of publication | Unsymmetrical NCN-pincer mononuclear and dinuclear nickel(ii) complexes of N-heterocyclic carbene (NHC): synthesis, structure and catalysis for Suzuki-Miyaura cross-coupling. |
Authors of publication | Gu, Shaojin; Du, Jiehao; Huang, Jingjing; Guo, Yun; Yang, Ling; Xu, Weilin; Chen, Wanzhi |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2017 |
Journal volume | 46 |
Journal issue | 2 |
Pages of publication | 586 - 594 |
a | 7.4549 ± 0.001 Å |
b | 9.4911 ± 0.0015 Å |
c | 15.3162 ± 0.0019 Å |
α | 85.011 ± 0.002° |
β | 80.161 ± 0.001° |
γ | 77.48 ± 0.001° |
Cell volume | 1041 ± 0.3 Å3 |
Cell temperature | 298 ± 2 K |
Ambient diffraction temperature | 298 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0968 |
Residual factor for significantly intense reflections | 0.0572 |
Weighted residual factors for significantly intense reflections | 0.1399 |
Weighted residual factors for all reflections included in the refinement | 0.1696 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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