Crystallography Open Database

Information card for entry 7041462

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Coordinates	7041462.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C126.5 H164 B4 La4 N8 Si4
Calculated formula	C126.5 H164 B4 La4 N8 Si4
Title of publication	Rare-earth metal hydrides supported by silicon-bridged boratabenzene fluorenyl ligands: synthesis, structure and reactivity.
Authors of publication	Wang, Chunhong; Xiang, Li; Leng, Xuebing; Chen, Yaofeng
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2017
Journal volume	46
Journal issue	4
Pages of publication	1218 - 1227
a	18.7173 ± 0.0014 Å
b	19.5181 ± 0.0014 Å
c	21.7889 ± 0.0016 Å
α	64.072 ± 0.001°
β	67.221 ± 0.001°
γ	86.825 ± 0.001°
Cell volume	6537.9 ± 0.8 Å³
Cell temperature	140 ± 2 K
Ambient diffraction temperature	140.15 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0688
Residual factor for significantly intense reflections	0.0473
Weighted residual factors for significantly intense reflections	0.1292
Weighted residual factors for all reflections included in the refinement	0.1417
Goodness-of-fit parameter for all reflections included in the refinement	0.988
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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