Information card for entry 7041632

Structure parameters

• Formula: C24 H30 Br3.03 F0.97 Si4
• Calculated formula: C24 H30 Br3.0255 F0.9745 Si4
• Title of publication: Tridentate Lewis-acids based on triphenylsilane.
• Authors of publication: Tomaschautzky, Janek; Neumann, Beate; Stammler, Hans-Georg; Mix, Andreas; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 5
• Pages of publication: 1645 - 1659
• a: 10.21572 ± 0.00013 Å
• b: 11.13196 ± 0.00015 Å
• c: 13.90239 ± 0.00016 Å
• α: 98.4221 ± 0.001°
• β: 103.528 ± 0.0011°
• γ: 104.87 ± 0.0012°
• Cell volume: 1449.33 ± 0.03 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0249
• Residual factor for significantly intense reflections: 0.0244
• Weighted residual factors for significantly intense reflections: 0.0629
• Weighted residual factors for all reflections included in the refinement: 0.0632
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No