Crystal structures and intense luminescence of tris(3-(2'-pyridyl)-pyrazolyl)borate Tb(3+) and Eu(3+) complexes with carboxylate co-ligands.
Authors of publication
Mikhalyova, Elena A.; Yakovenko, Anastasiya V.; Zeller, Matthias; Gavrilenko, Konstantin S.; Kiskin, Mikhail A.; Smola, Sergey S.; Dotsenko, Vladimir P.; Eremenko, Igor L.; Addison, Anthony W.; Pavlishchuk, Vitaly V.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2017
Journal volume
46
Journal issue
11
Pages of publication
3457 - 3469
a
41.836 ± 0.005 Å
b
10.1087 ± 0.0013 Å
c
19.224 ± 0.002 Å
α
90°
β
91.616 ± 0.002°
γ
90°
Cell volume
8126.7 ± 1.7 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
7
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0731
Residual factor for significantly intense reflections
0.0593
Weighted residual factors for significantly intense reflections
0.1221
Weighted residual factors for all reflections included in the refinement
0.1291
Goodness-of-fit parameter for all reflections included in the refinement