Information card for entry 7042022

Structure parameters

• Formula: C24 H32 I2 N4 Pd
• Calculated formula: C24 H32 I2 N4 Pd
• Title of publication: Chelated bis(NHC) complexes of saturated (imidazolin-2-ylidene) NHC ligands: structural authentication and facile ligand fragmentation.
• Authors of publication: Gardiner, Michael G.; McGuinness, David S.; Vanston, Catriona R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 9
• Pages of publication: 3051 - 3058
• a: 8.8558 ± 0.0002 Å
• b: 11.7308 ± 0.0003 Å
• c: 14.0161 ± 0.0004 Å
• α: 68.898 ± 0.001°
• β: 87.959 ± 0.001°
• γ: 75.968 ± 0.001°
• Cell volume: 1315.74 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 99.89 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0294
• Residual factor for significantly intense reflections: 0.0277
• Weighted residual factors for significantly intense reflections: 0.0699
• Weighted residual factors for all reflections included in the refinement: 0.0708
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No