Information card for entry 7042057

Structure parameters

• Formula: C57 H48 Mo N8 O3 P2
• Calculated formula: C57 H48 Mo N8 O3 P2
• Title of publication: 5-(2-Pyridil)-1H-tetrazole complexes with Mo(iv) and W(iv) cyanides.
• Authors of publication: Mrowiec, A.; Jurowska, A.; Hodorowicz, M.; Szklarzewicz, J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 12
• Pages of publication: 4030 - 4037
• a: 13.3538 ± 0.0006 Å
• b: 13.5304 ± 0.0005 Å
• c: 16.6261 ± 0.0007 Å
• α: 71.257 ± 0.004°
• β: 88.524 ± 0.004°
• γ: 62.823 ± 0.004°
• Cell volume: 2504.4 ± 0.2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1398
• Residual factor for significantly intense reflections: 0.1003
• Weighted residual factors for significantly intense reflections: 0.1828
• Weighted residual factors for all reflections included in the refinement: 0.1972
• Goodness-of-fit parameter for all reflections included in the refinement: 1.227
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No