Information card for entry 7042063

Structure parameters

• Formula: C23 H45 Cl2 Ge N3 O0.5 Si2 Sn
• Calculated formula: C23 H45 Cl2 Ge N3 O0.5 Si2 Sn
• Title of publication: Reactivity of an amidinato silylene and germylene toward germanium(ii), tin(ii) and lead(ii) halides.
• Authors of publication: Shan, Yu-Liang; Leong, Bi-Xiang; Xi, Hong-Wei; Ganguly, Rakesh; Li, Yongxin; Lim, Kok Hwa; So, Cheuk-Wai
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 11
• Pages of publication: 3642 - 3648
• a: 9.0571 ± 0.0005 Å
• b: 11.1854 ± 0.0006 Å
• c: 16.83 ± 0.001 Å
• α: 107.251 ± 0.002°
• β: 91.186 ± 0.002°
• γ: 104.147 ± 0.002°
• Cell volume: 1570.91 ± 0.15 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0708
• Residual factor for significantly intense reflections: 0.0442
• Weighted residual factors for significantly intense reflections: 0.0874
• Weighted residual factors for all reflections included in the refinement: 0.0976
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No