Crystallography Open Database

Information card for entry 7042072

7042071 << 7042072 >> 7042073

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Coordinates	7042072.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	16139_Complex-2-CH3
Formula	C46 H69 Ga N4 P3 Rh
Calculated formula	C46 H69 Ga N4 P3 Rh
Title of publication	Structure and dynamic NMR behavior of rhodium complexes supported by Lewis acidic group 13 metallatranes.
Authors of publication	Moore, James T.; Smith, Nicholas E.; Lu, Connie C.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2017
Journal volume	46
Journal issue	17
Pages of publication	5689 - 5701
a	12.3557 ± 0.0013 Å
b	13.1544 ± 0.0014 Å
c	14.8942 ± 0.0016 Å
α	72.211 ± 0.001°
β	79.601 ± 0.001°
γ	81.319 ± 0.001°
Cell volume	2255.3 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0463
Residual factor for significantly intense reflections	0.0335
Weighted residual factors for significantly intense reflections	0.0726
Weighted residual factors for all reflections included in the refinement	0.0789
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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