Information card for entry 7042264

Structure parameters

• Formula: C44 H52 I2 Mg2 N2 O2 Si2
• Calculated formula: C44 H52 I2 Mg2 N2 O2 Si2
• SMILES: c12cccc3c1c(ccc3)[N]1([Mg](I)([N]2([Si](C)(c2ccccc2)c2ccccc2)[Mg]1(I)[O](CC)CC)[O](CC)CC)[Si](C)(c1ccccc1)c1ccccc1
• Title of publication: 1,8-Bis(silylamido)naphthalene complexes of magnesium and zinc synthesised through alkane elimination reactions.
• Authors of publication: Bradley, Mark A.; Birchall, Chris; Blake, Alexander J.; Lewis, William; Moxey, Graeme J.; Kays, Deborah L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 12
• Pages of publication: 4101 - 4110
• a: 20.2536 ± 0.0007 Å
• b: 10.19 ± 0.0003 Å
• c: 21.7038 ± 0.0007 Å
• α: 90°
• β: 93.943 ± 0.003°
• γ: 90°
• Cell volume: 4468.7 ± 0.2 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0508
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1465
• Weighted residual factors for all reflections included in the refinement: 0.1473
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No