Information card for entry 7042369

Structure parameters

• Formula: C33 H62 Ga2 P2 Si2
• Calculated formula: C33 H62 Ga2 P2 Si2
• Title of publication: Synthesis of heteroatomic bridged paracyclophanes.
• Authors of publication: Reuter, K.; Maas, R. G. M.; Reuter, A.; Kilgenstein, F.; Asfaha, Y.; von Hänisch, C
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 14
• Pages of publication: 4530 - 4541
• a: 11.4453 ± 0.0007 Å
• b: 13.4431 ± 0.0009 Å
• c: 14.5944 ± 0.0008 Å
• α: 67.504 ± 0.002°
• β: 68.993 ± 0.002°
• γ: 88.105 ± 0.002°
• Cell volume: 1922.6 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0491
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.0655
• Weighted residual factors for all reflections included in the refinement: 0.0707
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No