Information card for entry 7042464

Structure parameters

• Formula: C29 H59 B Cl6 N2 Zr2
• Calculated formula: C29 H57 B Cl6 N2 Zr2
• Title of publication: Isolable zirconium hydride species in the reaction of amido complexes with amine-boranes.
• Authors of publication: Greño, Maider; Mena, Miguel; Pérez-Redondo, Adrián; Yélamos, Carlos
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 16
• Pages of publication: 5138 - 5142
• a: 16.301 ± 0.016 Å
• b: 20.61 ± 0.004 Å
• c: 48.31 ± 0.04 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 16230 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 70
• Hermann-Mauguin space group symbol: F d d d :2
• Hall space group symbol: -F 2uv 2vw
• Residual factor for all reflections: 0.0705
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.0945
• Weighted residual factors for all reflections included in the refinement: 0.104
• Goodness-of-fit parameter for all reflections included in the refinement: 1.115
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No