Information card for entry 7042514

Structure parameters

• Formula: C43 H42 Cl N O4 P2 Ru Si
• Calculated formula: C43 H42 Cl N O4 P2 Ru Si
• Title of publication: Highly selective synthesis of substituted (E)-alkenylsilatranes via catalytic trans-silylation and mechanistic implications.
• Authors of publication: Sztorch, Bogna; Frąckowiak, Dawid; Pyziak, Jadwiga; Czapik, Agnieszka; Hoffmann, Marcin; Marciniec, Bogdan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 15
• Pages of publication: 4975 - 4981
• a: 9.6141 ± 0.0003 Å
• b: 12.1035 ± 0.0004 Å
• c: 18.1419 ± 0.0005 Å
• α: 94.833 ± 0.002°
• β: 100.853 ± 0.002°
• γ: 104.855 ± 0.002°
• Cell volume: 1984.39 ± 0.11 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.0898
• Weighted residual factors for all reflections included in the refinement: 0.0945
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No