Information card for entry 7042569

Structure parameters

• Formula: C68 H50 Ho2
• Calculated formula: C68 H50 Ho2
• Title of publication: Methylene-bridged, intramolecular donor-acceptor systems based on rare-earth metals and phosphinomethanides.
• Authors of publication: Pieper, Martin; Lamm, Jan-Hendrik; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 16
• Pages of publication: 5326 - 5336
• a: 11.59946 ± 0.00011 Å
• b: 14.4403 ± 0.00017 Å
• c: 15.36988 ± 0.00011 Å
• α: 90°
• β: 96.7876 ± 0.0008°
• γ: 90°
• Cell volume: 2556.41 ± 0.04 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0489
• Residual factor for significantly intense reflections: 0.0476
• Weighted residual factors for significantly intense reflections: 0.1171
• Weighted residual factors for all reflections included in the refinement: 0.1184
• Goodness-of-fit parameter for all reflections included in the refinement: 1.129
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No