Information card for entry 7042751

Structure parameters

• Formula: C69 H96 Ge9 K4 N6 O39 W3
• Calculated formula: C69 H96 Ge9 K4 N6 O39 W3
• Title of publication: [Ge9{M(CO)5}3]4-: Electrophilic Addition of M(CO)5 and [E9]4- Zintl anions (M = Cr, Mo, W) †
• Authors of publication: Wang, LuLu; Wang, Yi; li, zhenyu; Ruan, Huapeng; Xu, Li
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 19.7716 ± 0.0009 Å
• b: 19.7716 ± 0.0009 Å
• c: 16.5975 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5619 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 176
• Hermann-Mauguin space group symbol: P 63/m
• Hall space group symbol: -P 6c
• Residual factor for all reflections: 0.0681
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for significantly intense reflections: 0.1277
• Weighted residual factors for all reflections included in the refinement: 0.1296
• Goodness-of-fit parameter for all reflections included in the refinement: 1.184
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No