Information card for entry 7043042

Structure parameters

• Formula: C31 H49 Ga N2 P Si
• Calculated formula: C30.997 H49 Ga N2 P Si
• Title of publication: Improved reactivity of a cyclic 13/15 compound by increased steric demand
• Authors of publication: Balmer, Markus; Kapitein, Manuel; von Hänisch, Carsten
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 9.9548 ± 0.0005 Å
• b: 12.7363 ± 0.0006 Å
• c: 14.9374 ± 0.0007 Å
• α: 75.424 ± 0.002°
• β: 87.916 ± 0.002°
• γ: 69.4 ± 0.002°
• Cell volume: 1712.87 ± 0.15 ų
• Cell temperature: 240 K
• Ambient diffraction temperature: 240 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0461
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0978
• Weighted residual factors for all reflections included in the refinement: 0.1029
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No